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Please use this identifier to cite or link to this item:
http://krishi.icar.gov.in/jspui/handle/123456789/38652
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DC Field | Value | Language |
---|---|---|
dc.contributor.author | Patil R., Khan Z., Pudale A., Shinde R., Shabeer A., Patil A., Banerjee Kaushik | en_US |
dc.date.accessioned | 2020-07-31T06:26:39Z | - |
dc.date.available | 2020-07-31T06:26:39Z | - |
dc.date.issued | 2018-10-16 | - |
dc.identifier.citation | Patil R., Khan Z., Pudale A., Shinde R., Shabeer A., Patil A., Banerjee Kaushik (2018). Comprehensive multiresidue determination of pesticides and plant growth regulators in grapevine leaves using liquid- and gas chromatography with tandem mass spectrometry. Journal of Chromatography A 1579: 73-82 | en_US |
dc.identifier.uri | https://www.sciencedirect.com/science/article/abs/pii/S0021967318312883?via%3Dihub | - |
dc.identifier.uri | http://krishi.icar.gov.in/jspui/handle/123456789/38652 | - |
dc.description | Not Available | en_US |
dc.description.abstract | Grape leaf, which is known for its nutritional and medicinal properties, is finding increased applications for cuisine and remedial purposes. This article reports a comprehensive analytical method for the identification and quantification of a broad range of pesticides and plant growth regulators (PGRs) in the grape leaf matrix. The sample preparation method for pesticides involved an optimized QuEChERS-based extraction protocol, with subsequent clean-up by the dispersive solid phase extraction (dSPE) using a mixture of sorbents (25 mg PSA + 5 mg GCB + 150 mg MgSO4). The PGRs were extracted with methanol. The performance of the method was investigated and validated for a mixture of 363 pesticides (148 in GC–MS/MS and 203 in LC–MS/MS) and 12 PGRs (LC–MS/MS) in compliance with the analytical quality control criteria of the SANTE/11813/2017 guidelines. The matrix effects were comparatively higher against grape berries. The findings indicated satisfactory recoveries at 10 ng/g and higher levels with precision RSDs less than 20%. This method has potential applications in commercial residue testing laboratories and also for the regulatory compliance check purposes for its lower LOQs compared to the corresponding EU-MRLs. | en_US |
dc.description.sponsorship | Not Available | en_US |
dc.language.iso | English | en_US |
dc.publisher | Elsevier | en_US |
dc.relation.ispartofseries | Not Available; | - |
dc.subject | Multiresidue analysis in grape leaf | en_US |
dc.subject | Pesticides and plant growth regulators | en_US |
dc.subject | GC-MS/MS | en_US |
dc.subject | LC-MS/MS | en_US |
dc.subject | Method validation | en_US |
dc.title | Comprehensive multiresidue determination of pesticides and plant growth regulators in grapevine leaves using liquid- and gas chromatography with tandem mass spectrometry | en_US |
dc.title.alternative | Not Available | en_US |
dc.type | Journal | en_US |
dc.publication.projectcode | Not Available | en_US |
dc.publication.journalname | Journal of Chromatography A | en_US |
dc.publication.volumeno | 1579 | en_US |
dc.publication.pagenumber | 73-82 | en_US |
dc.publication.divisionUnit | National Reference Laboratory | en_US |
dc.publication.sourceUrl | https://doi.org/10.1016/j.chroma.2018.10.025 | en_US |
dc.publication.authorAffiliation | ICAR::National Research Centre for Grapes | en_US |
dc.ICARdataUseLicence | http://krishi.icar.gov.in/PDF/ICAR_Data_Use_Licence.pdf | en_US |
dc.publication.naasrating | 10.05 | en_US |
Appears in Collections: | HS-NRCG-Publication |
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