Nonlinear spin wave magnetization of solution synthesized Ni nanoparticles
DSpace at IIT Bombay
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Title |
Nonlinear spin wave magnetization of solution synthesized Ni nanoparticles
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Creator |
VITTA, S
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Subject |
molecular-beams
particles nickel microstructure clusters fe co |
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Description |
The magnetic properties of Ni nanoparticles synthesized using a soft chemical method followed by heat treatment in H-2 atmosphere have been studied in detail. The powder consists of pure Ni with no additional phase and the average crystallite size is 30 +/- 5 nm, determined using the modified Scherer relation. The crystallites tend to agglomerate into large particles of sizes 50-100 nm, as observed by transmission electron microscopy. The saturation magnetization is found to be 46.42 emu g(-1) at 5 K, about 80% of the bulk magnetization value. The temperature dependence of saturation magnetization for T < 0.5T(C) is found to deviate from the linear Bloch's T-3/2 law indicating that spin wave interactions needs to be considered to understand the behavior. The spin wave stiffness constant obtained by fitting the saturation magnetization decay to a nonlinear spin wave model is lower by an order of magnitude compared to that of bulk Ni. The coercivity on the other hand decreases from 67 Oe at 5 K to 36 Oe at 300 K with a temperature dependence slower than the T-1/2 behavior predicted for noninteracting superparamagnetic particles. (c) 2007
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Publisher |
AMER INST PHYSICS
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Date |
2011-07-16T10:04:56Z
2011-12-26T12:49:42Z 2011-12-27T05:35:19Z 2011-07-16T10:04:56Z 2011-12-26T12:49:42Z 2011-12-27T05:35:19Z 2007 |
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Type |
Article
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Identifier |
JOURNAL OF APPLIED PHYSICS, 101(6), -
0021-8979 http://dx.doi.org/10.1063/1.2710437 http://dspace.library.iitb.ac.in/xmlui/handle/10054/4398 http://hdl.handle.net/10054/4398 |
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Language |
en
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