Single crystalline nickel nanorods inside carbon nanotubes: Growth behavior, structure, and magnetic properties
DSpace at IIT Bombay
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Title |
Single crystalline nickel nanorods inside carbon nanotubes: Growth behavior, structure, and magnetic properties
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Creator |
TYAGI, PK
MISRA, A SINGH, MK TITUS, E MISRA, DS GHATAK, J SATYAM, PV ROY, M |
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Subject |
field emitters
nanowires nanocomposites temperature fabrication templates films size ni carbon nanotubes nickel nanorods magnetic properties lattice fringes |
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Description |
Nickel nanorods with diameters ranging from 5 to 10 nm, encapsulated inside the carbon nanotubes, are prepared using microwave plasma chemical vapor deposition. High-resolution transmission electron microscopy (HRTEM) studies reveal the perfect crystalline nature of the rods with of-spacing closely matching the (1111) interplanar spacing of Ni. The (1111) planes of the Ni nanorods are always aligned at 39.6° with respect to the graphite planes of the nanotubes. The cosine component of the d-spacing along the direction of the graphite planes is found to be 1.6 &ANGS;; exactly half the d-spacing between the graphite planes. The electron diffraction pattern shows clear spots corresponding to Ni structure. The field cooled and zero field cooled magnetization data reveal the reversibility of the magnetization of the Ni nanorods and show a blocking temperature of 195 K, which correspond to energy barrier of 0.4 eV/(V).
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Publisher |
AMER SCIENTIFIC PUBLISHERS
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Date |
2011-07-17T03:55:35Z
2011-12-26T12:50:06Z 2011-12-27T05:36:05Z 2011-07-17T03:55:35Z 2011-12-26T12:50:06Z 2011-12-27T05:36:05Z 2005 |
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Type |
Article
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Identifier |
JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 5(4), 596-600
1533-4880 http://dx.doi.org/10.1166/jnn.2005.070 http://dspace.library.iitb.ac.in/xmlui/handle/10054/4607 http://hdl.handle.net/10054/4607 |
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Language |
en
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