Some Mechanistic Insights into the Gelation of Regenerated Silk Fibroin Sol
DSpace at IIT Bombay
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Title |
Some Mechanistic Insights into the Gelation of Regenerated Silk Fibroin Sol
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Creator |
NAGARKAR, S
PATIL, A LELE, A BHAT, S BELLARE, J MASHELKAR, RA |
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Subject |
bombyx-mori
in-vitro rheological behavior hydrogels gene biomaterials scaffolds rheometry proteins gland |
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Description |
We provide some new insights into the kinetics and mechanism of sol-gel transition as it pertains to regenerated silk fibroin, which is the principle structural protein of silkworm silk fiber. Silk fibroin was dissolved in lithium bromide and dialyzed against deionized water to prepare a regenerated fibroin solution. This solution was found to be unstable at lower pH and transformed into a colloidal gel. The kinetics and mechanism of the sol-gel transition were investigated using rheology and light scattering. We show that gelation proceeds in two steps. In the first step, a weak gel is formed almost immediately upon lowering the pH, while in the second step further gelation proceeds rapidly after a long induction time to form a self-similar structure.
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Publisher |
AMER CHEMICAL SOC
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Date |
2011-07-14T21:03:56Z
2011-12-26T12:47:38Z 2011-12-27T05:37:32Z 2011-07-14T21:03:56Z 2011-12-26T12:47:38Z 2011-12-27T05:37:32Z 2009 |
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Type |
Article
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Identifier |
INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 48(17), 8014-8023
0888-5885 http://dx.doi.org/10.1021/ie801723f http://dspace.library.iitb.ac.in/xmlui/handle/10054/4068 http://hdl.handle.net/10054/4068 |
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Language |
en
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