ACETYLENIC DERIVATIVES OF FE-2(CO)(6)(MU-SE-2) - SYNTHESIS AND SPECTROSCOPIC CHARACTERIZATION OF [(CO)(6)FE-2(MU-SEC(H)=C(H)SE)] AND [((CO)(6)FE2SE2)(2)(MU-C(H)-C(H))]
DSpace at IIT Bombay
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Title |
ACETYLENIC DERIVATIVES OF FE-2(CO)(6)(MU-SE-2) - SYNTHESIS AND SPECTROSCOPIC CHARACTERIZATION OF [(CO)(6)FE-2(MU-SEC(H)=C(H)SE)] AND [((CO)(6)FE2SE2)(2)(MU-C(H)-C(H))]
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Creator |
MATHUR, P
DASH, AK HOSSAIN, MM SATYANARAYANA, CVV |
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Subject |
bond reduction
clusters complexes ligands fe2(co)6(mu-se2) se te iron selenium |
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Description |
The new acetylenic derivatives [(CO)(6)Fe-2{mu-SeC(H)=C(H)Se}] and [{(CO)(6)Fe2Se2}(2){mu-C(H)-C(H)}] have been isolated from the room-temperature reaction of Fe-2(CO)(6)(mu-Se-2) with acetylene in methanol solvent containing sodium acetate. The products have been characterized by IR and H-1, C-13 and Se-77 NMR spectroscopy. The NMR spectroscopic features of the related phenylacetylene derivatives[(CO)(6)Fe-2{mu-SeC(Ph)=C(H)Se}] and [{(CO)(6)Fe2Se2}(2){mu-C(Ph)-C(H)}] are also reported.
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Publisher |
ELSEVIER SCIENCE SA LAUSANNE
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Date |
2011-07-29T03:10:06Z
2011-12-26T12:47:43Z 2011-12-27T05:38:57Z 2011-07-29T03:10:06Z 2011-12-26T12:47:43Z 2011-12-27T05:38:57Z 1995 |
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Type |
Article
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Identifier |
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 493(1-2), 257-260
0022-328X http://dx.doi.org/10.1016/0022-328X(94)05350-K http://dspace.library.iitb.ac.in/xmlui/handle/10054/7562 http://hdl.handle.net/10054/7562 |
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Language |
en
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