SOLVENT-EXTRACTION SEPARATION OF CESIUM WITH DIBENZO-24-CROWN-8 FROM PICRATE SOLUTION
DSpace at IIT Bombay
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Title |
SOLVENT-EXTRACTION SEPARATION OF CESIUM WITH DIBENZO-24-CROWN-8 FROM PICRATE SOLUTION
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Creator |
VIBHUTE, RG
KHOPKAR, SM |
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Subject |
metal picrates
univalent |
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Description |
Cesium (25-mu-g) was extracted with 0.03M DB-24-crown-8 at pH 3.0 from 0.01M picric acid in the presence of 2 ml methanol. It was stripped with 3M perchloric acid and was determined by atomic absorption spectrophotometry. The nature of the extracted species was 1:1:1. Dichloromethane was a suitable diluent. Nitric and perchloric acid were the best stripping agents. Cesium was not only separated from alkali and alkaline earth elements but also from zirconium, hafnium, thorium, usually present in fission products. The method is applicable for determination of cesium from real samples.
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Publisher |
AKADEMIAI KIADO
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Date |
2011-07-12T20:31:10Z
2011-12-26T12:47:49Z 2011-12-27T05:40:31Z 2011-07-12T20:31:10Z 2011-12-26T12:47:49Z 2011-12-27T05:40:31Z 1991 |
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Type |
Article
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Identifier |
JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY-ARTICLES, 152(2), 487-496
0236-5731 http://dx.doi.org/10.1007/BF02104701 http://dspace.library.iitb.ac.in/xmlui/handle/10054/3617 http://hdl.handle.net/10054/3617 |
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Language |
en
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