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Characterization and conformational studies of a novel trinitro steroid using 2D-NMR

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Title Characterization and conformational studies of a novel trinitro steroid using 2D-NMR
 
Creator KATOCH, R
SRIDHARAN, R
TRIVEDI, GK
 
Subject nuclear-magnetic-resonance
fast atom bombardment
mass-spectrometry
ion-source
solids
 
Description Conformational analysis of nitro substituted 4-en-3-one steroids has been further investigated using high resolution 2D-NMR techniques. An attempt on the preparation of 6 beta-nitrocholest-4-en-3-one resulted in a new trinitro steroid, 2,2,6 beta-trinitrocholest-4-en-3-one. These compounds have been characterized using COSY, HETCOR, NOESY experiments and the probable pathways to these products have been discussed.
 
Publisher INDIAN CHEMICAL SOC
 
Date 2011-08-02T10:47:53Z
2011-12-26T12:53:51Z
2011-12-27T05:40:55Z
2011-08-02T10:47:53Z
2011-12-26T12:53:51Z
2011-12-27T05:40:55Z
1998
 
Type Article
 
Identifier JOURNAL OF THE INDIAN CHEMICAL SOCIETY, 75(10-12), 543-547
0019-4522
http://dspace.library.iitb.ac.in/xmlui/handle/10054/8767
http://hdl.handle.net/10054/8767
 
Language en