CVD synthesis of carbon nanotubes using a finely dispersed cobalt catalyst and their use in double layer electrochemical capacitors
DSpace at IIT Bombay
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Title |
CVD synthesis of carbon nanotubes using a finely dispersed cobalt catalyst and their use in double layer electrochemical capacitors
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Creator |
CHATTERJEE, AK
SHARON, M BANERIEE, R NEUMANN-SPALLART, M |
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Subject |
chemical-vapor-deposition
fullerene tubules supercapacitor electrodes nanobeads camphor carbon nanotube cvd synthesis double layer capacitor turpentine oil |
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Description |
Carbon nanotubes (CNT) were obtained by chemical vapour deposition (CVD), decomposing turpentine oil over finely dispersed Co metal as a catalyst at 675 degreesC. Scanning electron microscope (SEM) and transmission electron microscope (TEM) images reveal that the nanotubes are densely packed and of 10-50 nm in diameter. The XRD pattern of purified CNT shows that they are graphitic in nature. Resistivity measurements of these CNT indicate that they are highly conducting. Hall measurements of CNT reveal that electrons are the majority carriers with a carrier concentration of 1.35 X 10(20) cm(-3). Cyclic voltammetry (CV) and constant current charging/discharging was used to characterise the behaviour of electrochemical double layer capacitors of purified CNT with H2SO4. For CNT/2 M H2SO4/CNT, a capacitance of 12 F g(-1) (based on the weight of the active material) was obtained. (C) 2003
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Publisher |
PERGAMON-ELSEVIER SCIENCE LTD
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Date |
2011-08-23T23:21:40Z
2011-12-26T12:56:39Z 2011-12-27T05:45:42Z 2011-08-23T23:21:40Z 2011-12-26T12:56:39Z 2011-12-27T05:45:42Z 2003 |
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Type |
Article
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Identifier |
ELECTROCHIMICA ACTA, 48(23), 3439-3446
0013-4686 http://dx.doi.org/10.1016/S0013-4686(03)00427-4 http://dspace.library.iitb.ac.in/xmlui/handle/10054/10685 http://hdl.handle.net/10054/10685 |
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Language |
en
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