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First crystallographic evidence for the formation of β-D-ribopyranosylamine from the reaction of ammonia with of D-ribose

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Title First crystallographic evidence for the formation of β-D-ribopyranosylamine from the reaction of ammonia with of D-ribose
 
Creator GUDNEPPANAVAR, RAJSEKHAR
RAO, CHEBROLU P
GUIONNEAU, PHILIPPE
 
Subject crystallography
hydrogen bonds
synthesis (chemical)
x-ray diffraction
 
Description β-D-Ribopyranosylamine was synthesized and characterized using analytical, spectral and single-crystal X-ray diffraction methods. The molecule exists in the chair form with the 4C1 conformation. The β anomeric form of C-1 is supported by the dihedral angles. The molecule exhibits both intra- and intermolecular hydrogen-bond interactions of the type O—H...O, N—H...O and C—H...O, and these are interconnected to each other to form chains.
 
Publisher Elsevier
 
Date 2009-02-27T11:09:26Z
2011-11-25T18:07:05Z
2011-12-26T13:06:44Z
2011-12-27T05:54:44Z
2009-02-27T11:09:26Z
2011-11-25T18:07:05Z
2011-12-26T13:06:44Z
2011-12-27T05:54:44Z
2003
 
Type Article
 
Identifier Carbohydrate Research 338(8), 801-805
0008-6215
http://dx.doi.org/10.1016/S0008-6215(03)00006-5
http://hdl.handle.net/10054/812
http://dspace.library.iitb.ac.in/xmlui/handle/10054/812
 
Language en