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Synthesis and X-ray crystal structure of a novel long chain acyclic phosphazene, N,N′-{dimethyl-bis(diphenylphosphiniminophosphorane)}ethylenediamine {(PhO)2P(O)N=PN(CH3)CH2}2, obtained via a Staudinger reaction

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Title Synthesis and X-ray crystal structure of a novel long chain acyclic phosphazene, N,N′-{dimethyl-bis(diphenylphosphiniminophosphorane)}ethylenediamine {(PhO)2P(O)N=PN(CH3)CH2}2, obtained via a Staudinger reaction
 
Creator BALAKRISHNA, MS
ABHYANKAR, RITA M
WALAWALKAR, MRINALINI G
 
Subject phosphazene
phosphinimines
staudinger reaction
x-ray structure
 
Description The title compound was synthesized by the reaction of N,N′-dimethyl-N,N′-bis(diphenylphosphino)ethylenediamine with phosphoryl azide and characterized by mass spectrometry, microanalysis, and 31P and 1H NMR spectroscopy and the structure was confirmed by single crystal X-ray studies.
 
Publisher Elsevier
 
Date 2009-03-20T05:57:24Z
2011-11-25T19:46:22Z
2011-12-26T13:07:39Z
2011-12-27T05:55:41Z
2009-03-20T05:57:24Z
2011-11-25T19:46:22Z
2011-12-26T13:07:39Z
2011-12-27T05:55:41Z
2001
 
Type Article
 
Identifier Tetrahedron Letters 42(14), 2733-2734
0040-4039
http://dx.doi.org/10.1016/S0040-4039(01)00236-2
http://hdl.handle.net/10054/1020
http://dspace.library.iitb.ac.in/xmlui/handle/10054/1020
 
Language en