Synthesis and properties of cyclophosphazenes appended with covalently linked porphyrin-ferrocene conjugates
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Title |
Synthesis and properties of cyclophosphazenes appended with covalently linked porphyrin-ferrocene conjugates
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Creator |
PAREEK, Y
RAVIKANTH, M |
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Subject |
Cyclophosphazenes
Porphyrin Ferrocene Conjugates Redox active Photo-induced electron transfer ELECTROCHEMICAL PROPERTIES ELECTRON-TRANSFER BORON-DIPYRRIN REDOX DENDRIMERS SCAFFOLDS RECOGNITION ASSEMBLIES ACTIVATION CHEMISTRY |
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Description |
Cyclotriphosphazene and cyclotetraphosphazene appended with six and eight covalently linked porphyrin-ferrocene conjugates respectively were synthesized by treating N3P3Cl6 and N4P4Cl8 with appropriate equivalents of ferrocene linked porphyrin containing meso-hydroxyphenyl group in THF in the presence of Cs2CO3 followed by column chromatographic purification. NMR and absorption studies indicated a weak interaction between adjacent porphyrin-ferrocene conjugates. Electrochemical studies supported electrochemical equivalence of ferrocenyl and porphyrinyl moieties in these multiporphyrin-ferrocene conjugate assemblies. The fluorescence studies showed significant quenching of porphyrin fluorescence due to photo-induced electron transfer from ferrocene to singlet state of porphyrin unit in these assemblies. (C) 2012 Elsevier B. V. All rights reserved.
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Publisher |
ELSEVIER SCIENCE SA
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Date |
2014-10-15T13:28:16Z
2014-10-15T13:28:16Z 2013 |
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Type |
Article
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Identifier |
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 72467-74
http://dx.doi.org/10.1016/j.jorganchem.2012.10.043 http://dspace.library.iitb.ac.in/jspui/handle/100/15004 |
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Language |
en
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