Bidirectional approach to Symmetrical spiro-1,3-bisketone via Grignard reaction and two fold ring-closing metathesis as key-steps
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Title |
Bidirectional approach to Symmetrical spiro-1,3-bisketone via Grignard reaction and two fold ring-closing metathesis as key-steps
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Creator |
KOTHA, S
ALI, R DIPAK, MK |
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Subject |
OLEFIN-METATHESIS
ACID-DERIVATIVES ENYNE METATHESIS CROSS-METATHESIS HETEROCYCLES ANNULATION ANALOGS Grignard reaction ring-closing metathesis spirocyclics 1,4-addition reaction |
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Description |
We have developed a useful method for the construction of symmetrical spiro-1,3-bisketone starting with a commercially available diethylmalonate by using double Grignard addition and two fold ring-closing metathesis as key steps. During the Grignard reaction, we observed 1,4-addition without involvement of copper catalyst.
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Publisher |
SCIENTIFIC PUBL-INDIA
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Date |
2016-01-15T10:54:53Z
2016-01-15T10:54:53Z 2015 |
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Type |
Article
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Identifier |
JOURNAL OF THE INDIAN CHEMICAL SOCIETY, 92(2)277-281
0019-4522 http://dspace.library.iitb.ac.in/jspui/handle/100/18399 |
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Language |
en
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