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Microstructural Stability of Fully Lamellar and Duplex y-TiAl Alloys During Creep

Electronic Theses of Indian Institute of Science

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Title Microstructural Stability of Fully Lamellar and Duplex y-TiAl Alloys During Creep
 
Creator Babu, R Prasath
 
Subject Titanium Alluminide Alloys
Titanium Alluminide Alloys - Creep
Titanium Alluminide Alloys - Microstructural Stability
Fully Lamellar Microstructure
Duplex Microstructure - Stabililty
Duplex Titanium Alluminide Alloys
Fully Lamellar Titanium Alluminide Alloys
γ-TiAl Alloys
Creep
Metallurgy
 
Description γ-TiAl based alloys have attracted considerable research interest in the past few decades and have gained niche high temperature applications in aero-engines and automobiles. As high temperature structural materials, these alloys require stable microstructures. This thesis aims at addressing knowledge gaps in the understanding of microstructural stability in two technologically important γ-TiAl based alloys in different microstructures, viz. fully lamellar (FL) and duplex. Creep and exposure tests were complemented with a variety of microstructural characterization tools (SEM, EBSD, TEM, XRD). Density functional theory based calculations were also performed to further the understanding of stability of phases. In the first part of the thesis, microstructural stability of a FL microstructure was studied under creep and high temperature exposure conditions. An aim of these studies was to probe the effect of stress orientation with respect to lamellar plates on microstructural changes during primary creep. It was observed that retention of excess α2 resulted in an unstable microstructure and so under stress and temperature, excess α2 was lost. However, depending on stress orientation, the sequence of precipitates formed was different. In particular, for certain stress orientations, the formation of the non-equilibrium C14 phase was observed. The stress dependence of microstructural evolution was found to be stem from internal stresses due to lattice misfit and elastic moduli mismatch between α2 and γ. In the second part of this thesis, microstructural stability of a duplex alloy was probed, with an emphasis on understanding mechanisms that lead to tertiary creep. The as-extruded microstructure consisted of bands of equiaxed grains and lamellar grains. During creep, loss of lamellar grains was observed and this was attended by kinking of laths and formation of dynamically recrystallized equiaxed grains. Significant dislocation activity was seen in both lamellar and equiaxed grains at all stages of creep. Initially, dislocation activity leads to strengthening and primary creep behavior, but at later stages, it triggers dynamic recrystallization. Dynamic recrystallization was found to be the rate controlling creep mechanism. Accelerating creep behavior was due to strain localization during the constant load tensile test resulting from microstructural instabilities such as kinking.
 
Contributor Karthikeyan, S
 
Date 2018-03-05T19:54:21Z
2018-03-05T19:54:21Z
2018-03-06
2012
 
Type Thesis
 
Identifier http://hdl.handle.net/2005/3234
http://etd.ncsi.iisc.ernet.in/abstracts/4095/G25497-Abs.pdf
 
Language en_US
 
Relation G25497