Identification, purification, and characterization of a secretory serine protease in an Indian strain of Leishmania donovani
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Title |
Identification, purification, and characterization of a secretory serine protease in an Indian strain of Leishmania donovani |
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Creator |
Choudhury, Rajdeep
Bhaumik, Siddhartha Kumar De, Tripti Chakraborti, Tapati |
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Subject |
Infectious Diseases and Immunology
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Description |
An aprotinin sensitive serine protease was identified in the culture supernatant of the Indian strain of Leishmania donovani (MHOM/IN/1983/AG83). The protease was subsequently purified and characterized. The apparent molecular mass of the enzyme was 115 kDa in SDS-PAGE under non-reducing condition, while on reduction it showed a 56 kDa protein band indicating that the protease is a dimeric protein. The purified enzyme was optimally active at the pH and temperature of 7.5 and 28�C, respectively. Assays of thermal stability indicated that the enzyme preserved 59% of activity even after pretreatment at 42�C for 1 h. The purified protease was not glycosylated and its isoelectric pI was 5.0. N-a-p-tosyl-Larginine methylester (TAME) appeared to be relatively better substrate among the commonly used synthetic substrates. The enzyme was inhibited by Ca2? and Mn2?, but activated by Zn2?. The protease could play important role(s) in the pathogenesis of visceral leishmaniasis or kala-azar. |
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Publisher |
Kluwer
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Date |
2009
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Type |
Article
PeerReviewed |
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Format |
application/pdf
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Identifier |
http://www.eprints.iicb.res.in/232/1/MOLECULAR_AND_CELLULAR_BIOCHEMISTRY%2C320%2C(1%2D2)%2C1%2D14%2C2009[129].pdf
Choudhury, Rajdeep and Bhaumik, Siddhartha Kumar and De, Tripti and Chakraborti, Tapati (2009) Identification, purification, and characterization of a secretory serine protease in an Indian strain of Leishmania donovani. Molecular and Cellular Biochemistry, 320 (1-2). 01-14. |
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Relation |
http://dx.doi.org/10.1007/s11010-008-9849-7
http://www.eprints.iicb.res.in/232/ |
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