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<strong>Reactivity of Electrochemically Synthesised Nano Zinc Wire in Facile Reduction of</strong><strong> Nitro and Azide Compounds</strong>

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Title Statement <strong>Reactivity of Electrochemically Synthesised Nano Zinc Wire in Facile Reduction of</strong><strong> Nitro and Azide Compounds</strong>
 
Added Entry - Uncontrolled Name Roy, Ujjal Kanti; Kazi Nazrul University
Financial support of this work by DST-New Delhi, SR/FT/CS-137/2011 dated 12.07.2012, and Science & Technology and Biotechnology-WB, 50(Sanc.)/ST/P/S&T/15G-10/2018 dated 30.01.2019 to UKR is gratefully acknowledged.
 
Uncontrolled Index Term electrochemistry, nano zinc, ZnCl2, ITO glass, FESEM, SQUID, Nitro, Azide, Amine, reduction.
 
Summary, etc. <p>Electrochemistry is used in generation of metallic nano zinc wire from aqueous zinc chloride. For this electrochemical process we designed a unit galvanic cell. During the electrochemical process both aliphatic and aromatic nitro and azide compounds undergo facile reduction to the corresponding amines. ZnCl<sub>2</sub> is used as stoichiometric reagent and causes electrochemical deposition of zinc in cathode. During the process wire shaped nano zinc architecture has been formed in cathode which is supposed to be the active reagent for reduction. The cathode deposited material has been characterised by powder XRD, XPS, FESEM, HRTEM, EDX, SQUID etc. The corresponding amines are prepared in good yields. Both zinc salts and aqueous solution can be recycled.</p>
 
Publication, Distribution, Etc. Indian Journal of Chemistry -Section A (IJCA)
2020-10-06 11:31:09
 
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http://op.niscair.res.in/index.php/IJCA/article/view/30938
 
Data Source Entry Indian Journal of Chemistry -Section A (IJCA); ##issue.vol## 59, ##issue.no## 8 (2020): INDIAN JOURNAL OF CHEMISTRY- SECTION A
 
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Nonspecific Relationship Entry http://op.niscair.res.in/index.php/IJCA/article/download/30938/465495052
http://op.niscair.res.in/index.php/IJCA/article/download/30938/465495053
http://op.niscair.res.in/index.php/IJCA/article/download/30938/465495054
http://op.niscair.res.in/index.php/IJCA/article/download/30938/465499835
http://op.niscair.res.in/index.php/IJCA/article/download/30938/0
http://op.niscair.res.in/index.php/IJCA/article/download/30938/465499852
 
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