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<strong>Synthesis and characterization of crystalline polyaniline</strong>

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Authentication Code dc
 
Title Statement <strong>Synthesis and characterization of crystalline polyaniline</strong>
 
Added Entry - Uncontrolled Name Singh, Bharti ; Fir author, as well as corresponding University Of Lucknow
Das, B
NO
 
Uncontrolled Index Term elementary particles and fields
AFM; Crystalline PANI; Crystals; TEM; XRD
 
Summary, etc. The present paper deals with the synthesis and characterization of crystalline polyaniline (PANI). In the present work the crystalline PANI was synthesized in two steps. Firstly, the amorphous polyaniline was prepared by co-precipitation method using aniline as precursor and ammonium peroxodisulfate as reagent. In second stage the crystalline PANI was prepared by the melting and slow cooling. Pellets of PANI were prepared at pressure of 3000-4000 kg/cm<sup>2</sup>. The resulting crystalline PANI was characterized by powder X-ray diffraction (PXRD), atomic force microscopy (AFM) and transmission electron microscopy (TEM). The PXRD pattern confirms the crystalline behaviour of PANI. The AFM results also support PXRD result due to presence of tiny crystals on the surface of PANI. TEM analysis reveals various nanorings connecting the characteristics diffraction spots of PANI nanoparticles.
 
Publication, Distribution, Etc. Indian Journal of Pure & Applied Physics (IJPAP)
2020-10-20 09:58:39
 
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http://op.niscair.res.in/index.php/IJPAP/article/view/25592
 
Data Source Entry Indian Journal of Pure & Applied Physics (IJPAP); ##issue.vol## 58, ##issue.no## 10 (2020): Indian Journal of Pure & Applied Physics
 
Language Note en
 
Nonspecific Relationship Entry http://op.niscair.res.in/index.php/IJPAP/article/download/25592/465479713
http://op.niscair.res.in/index.php/IJPAP/article/download/25592/465479714
http://op.niscair.res.in/index.php/IJPAP/article/download/25592/465479715
http://op.niscair.res.in/index.php/IJPAP/article/download/25592/465479716
 
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