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Ionic liquid-based microwave-assisted extraction of Heneicos-1-ene from coriander foliage and optimizing yield parameters by response surface methodology.

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Relation http://ir.cftri.com/14644/
https://doi.org/10.1080/10826068.2019.1687519
 
Title Ionic liquid-based microwave-assisted extraction
of Heneicos-1-ene from coriander foliage and
optimizing yield parameters by response surface
methodology.
 
Creator Siddharth, Priyadarshi
Manohar, B.
Madhava Naidu, M.
 
Subject 01 Analysis
16 Nutritive value
30 Spices/Condiments
 
Description In this study, an efficient ionic liquid (IL)-based microwave-assisted extraction (IL-MAE) was
employed for the extraction of Heneicos-1-ene from coriander foliage. Quantification of Heneicos1-ene was carried out using high-performance liquid chromatography. Parameters affecting extraction such as material to solvent ratio (1:10, 1:15, and 1:20), types of IL ([CH3(CH2)3]4NF,
[BMIM][PF6], [BMIM][BF4], and [C6H5]4P[Br]), concentration of IL (0.1, 0.5, and 1.0 M), microwave
power (200, 500, and 800 W), extraction temperature (50, 70, and 90 �C) and extraction time (2, 6,
and 10 min) were evaluated. Response surface methodology was applied to determine the optimum levels of these parameters to get maximum yield. The optimal conditions were achieved at
800 W, 90 �C for 2 min at a material to solvent ratio of 1:10 using 0.1 M solution of [BMIM][BF4], to
get maximum predicted yield of Heneicos-1-ene (412.8 mg/100 g) as against 408.5 ± 1.14 mg/100 g
for experimental value with 0.991 correlation coefficient. IL-MAE resulted in 5.85 times higher yield
as compared to the conventional method (69.77 ± 1.8 mg/100 g).
 
Publisher Taylor & Francis
 
Date 2020
 
Type Article
PeerReviewed
 
Format pdf
 
Language en
 
Identifier http://ir.cftri.com/14644/1/Preparative%20Biochemistry%20%26%20Biotechnology%202020.pdf
Siddharth, Priyadarshi and Manohar, B. and Madhava Naidu, M. (2020) Ionic liquid-based microwave-assisted extraction of Heneicos-1-ene from coriander foliage and optimizing yield parameters by response surface methodology. Preparative Biochemistry and Biotechnology, 50 (3). pp. 246-251. ISSN 1082-6068