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Preparation of complex polyol ester base oil for lubricant from cyclohexane oxidation waste water

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Title Preparation of complex polyol ester base oil for lubricant from cyclohexane oxidation waste water
 
Creator Mishra, Ananta Kumar
Valodkar, Mayur C
Vaishnav, Pujan B
 
Subject Base oil
Cyclohexane oxidation
Cyclohexanone
Lubricant
Polyol ester
 
Description 521-524
Oxidation of cyclohexane in air produces cyclohexanone and cyclohexanol in cyclopol-bis process along with waste water stream containing valuable carboxylic acids. Process is devised in this manuscript to prepare complex polyol ester base oil by utilizing the waste water. The waste water stream from the cyclohexane oxidation process of Gujarat state fertilizers and chemicals ltd. has been vacuum distilled with a vacuum of 700 mmHg to remove water followed by filtration to separate the solid and liquid fractions. The liquid fraction is reacted with diethylene glycol to synthesize complex polyol ester base oil for lubricant. The base oil so obtained has a kinematic viscosity of 113 cSt at 40°C, pour point of -33°C and viscosity index of 109.
 
Date 2021-02-02T07:05:59Z
2021-02-02T07:05:59Z
2020-11
 
Type Article
 
Identifier 0975-0991 (Online); 0971-457X (Print)
http://nopr.niscair.res.in/handle/123456789/56071
 
Language en_US
 
Rights CC Attribution-Noncommercial-No Derivative Works 2.5 India
 
Publisher NISCAIR-CSIR, India
 
Source IJCT Vol.27(6) [November 2020]