<p>Synthesis and crystal structure of a distorted face sharing double cubane like tetranuclear Ni<sup>II</sup>-Cu<sub>2</sub><sup>II</sup>-Ni<sup>II </sup>compound derived from a reduced di-Schiff base ligand</p>
Online Publishing @ NISCAIR
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Authentication Code |
dc |
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Title Statement |
<p>Synthesis and crystal structure of a distorted face sharing double cubane like tetranuclear Ni<sup>II</sup>-Cu<sub>2</sub><sup>II</sup>-Ni<sup>II </sup>compound derived from a reduced di-Schiff base ligand</p> |
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Added Entry - Uncontrolled Name |
Hazari, Alokesh ; Department of Chemistry, Government General Degree College, Singur 712 409, West Bengal, India |
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Uncontrolled Index Term |
Nickel(II), Copper(II), Tetranuclear, Reduced Schiff base, End-on azide |
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Summary, etc. |
<p style="text-align: justify;">One new tetranuclear face sharing distorted double cubane like hetero-metallic Ni<sup>II</sup><sub>2</sub>Cu<sub>2</sub><sup>II </sup>compound has been synthesized using a [NiL<sup>R</sup>] “metalloligand”, where H<sub>2</sub>L<sup>R</sup> = N,N'-bis(2-hydroxybenzyl)-1,3-propanediamine. The compound has been characterized by elemental analysis, spectroscopic methods and single crystal XRD. In the compound, in addition to the <em>m</em><sub>2</sub>-phenoxido bridges, the two terminal Ni<sup>II</sup> atoms are linked to each of the central Cu<sup>II</sup> ion by means of an end-on bridging azido (<em>m</em><sub>1,1</sub>-N<sub>3</sub>) ion separately, resulting a tetranuclear cubane like structure.</p> |
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Publication, Distribution, Etc. |
Indian Journal of Chemistry (IJC) 2022-05-31 17:21:39 |
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Electronic Location and Access |
application/pdf http://op.niscair.res.in/index.php/IJC/article/view/63634 |
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Data Source Entry |
Indian Journal of Chemistry (IJC); ##issue.vol## 61, ##issue.no## 5 (2022): Indian Journal of Chemistry-(IJC) |
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Language Note |
en |
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