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Simple approach for the synthesis of a 1,1'-(ethane-1,2 diylbis(azanediyl))bis(pentan-2-ol): <a href="https://www.sciencedirect.com/science/article/pii/0141813087900584"><sup>13</sup>C/<sup>1</sup>H NMR spectroscopy</a> and <a href="https://www.sciencedirect.com/science/article/pii/0921452693902496">electrical characterizatio</a>ns

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Title Statement Simple approach for the synthesis of a 1,1'-(ethane-1,2 diylbis(azanediyl))bis(pentan-2-ol): <a href="https://www.sciencedirect.com/science/article/pii/0141813087900584"><sup>13</sup>C/<sup>1</sup>H NMR spectroscopy</a> and <a href="https://www.sciencedirect.com/science/article/pii/0921452693902496">electrical characterizatio</a>ns
 
Added Entry - Uncontrolled Name Wechteti, Lassaad ; University of Tunis El Manar, Faculty of Sciences of Tunis, Chemistry Department, Laboratory of Structural Organic Chemistry, 2092 Tunis, Tunisia
Souemti, Ahmed ; University of Tunis El Manar, Faculty of Sciences of Tunis, Chemistry Department, LR19ES02 Applied Mineral Chemistry Laboratory (LCMA), 2092 Tunis, Tunisia
Selmi, Aymen ; University of Tunis El Manar, Faculty of Sciences of Tunis, Physics Department, LR99ES17 Laboratory of Materials Organisation and Properties, 2092 Tunis, Tunisia
Romdhani-Younes, Moufida ; University of Tunis El Manar, Faculty of Sciences of Tunis, Chemistry Department, Laboratory of Structural Organic Chemistry, 2092 Tunis, Tunisia
 
Uncontrolled Index Term β-Aminoalcohols, vibrational modes, activation energy, Arrhenius plot, dielectric properties
 
Summary, etc. <p style="text-align: justify;">1,1'-(Ethane-1,2-diylbis(azanediyl))bis(pentan-2-ol) a β-aminoalcohol material denoted as <strong>2a</strong> has been successfully synthesized. A white highly pure transparent material has been obtained after purification by chromatography techniques. Infrared spectroscopy has been used to identify the −NH and −OH functional groups. <sup>1</sup>H and <sup>13</sup>C NMR spectroscopy has confirmed the proposed structure. Complex Impedance Spectroscopy indicates an insulator behavior of the studied materials in the 313-393°C temperature range. Conductivity within this material is in intragrain contribution and its activation energy is about 1.3 eV. The physical properties of the studied material allow to consider β-amino alcohols as versatile intermediates for many organic compounds in the making of natural and synthetic originated biologically active compounds. They are widely used as β-blockers, insecticidal agents, and chiral auxiliaries.</p>
 
Publication, Distribution, Etc. Indian Journal of Chemistry (IJC)
2022-07-18 17:03:37
 
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http://op.niscair.res.in/index.php/IJC/article/view/64627
 
Data Source Entry Indian Journal of Chemistry (IJC); ##issue.vol## 61, ##issue.no## 7 (2022): Indian Journal of Chemistry-(IJC)
 
Language Note en