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Nano silica sulfuric acid catalyzed facile synthesis of azothiadiazoles under cogrinding and solvent-free technique

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Title Nano silica sulfuric acid catalyzed facile synthesis of azothiadiazoles under cogrinding and solvent-free technique
 
Creator Kambale, Varsha
Jadhav, Jagannath
Piste, Pravina
 
Subject Azo dyes
Nano silica sulfuric acid
Thiodiazole
Rice husk
Mortal-pestle grinding
 
Description 650-658
An efficient method for the use of nano silica sulfuric acid as a heterogeneous catalyst in the synthesis of thiadiazolecontaining
azo dyes via diazo coupling of substituted amino thiazole under solvent-free conditions is described. The method
presented is effective, green, inexpensive, and satisfactory to give the products in high yield with an excellent purity in short
times under mortar–pestle grinding. The environmental friendliness and re-usability of the catalyst make this protocol
attractive in organic synthesis.
 
Date 2022-07-05T10:36:57Z
2022-07-05T10:36:57Z
2022-06
 
Type Article
 
Identifier 2583-1321 (Online); 0019-5103 (Print)
http://nopr.niscpr.res.in/handle/123456789/60029
 
Language en
 
Publisher NIScPR-CSIR, India
 
Source IJC Vol.61(06) [June 2022]