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Solvent and catalyst free efficient chemoselective synthesis of 1,1-diacetate under visible light irradiation
NOPR - NISCAIR Online Periodicals Repository
View Archive Info| Field | Value | |
| Title |
Solvent and catalyst free efficient chemoselective synthesis of 1,1-diacetate under visible light irradiation
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| Creator |
Hote, Baliram S
Siddiqui, Tabassum A J Pisal, Parshuram M |
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| Subject |
1,1-Diacetate
Visible light Solvent- and catalyst free |
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| Description |
1184-1187
One of the synthetic intermediates is used in many organic transformations. A method for highly efficient synthesis of 1,1-diacetate (3a-j) from mixture of various substituted benzaldehydes and acetic anhydride under solvent- and catalyst free using visible light irradiation (150 W tungsten lamp) has been developed. The main advantages of this protocol includes shorter reaction time, eco-friendly, mild reaction condition, easy work-up procedures, high yields of products, are the attractive features of the present methodology. All synthesized 3a-j compounds were characterized by IR, 1H NMR and mass spectral analysis. |
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| Date |
2022-11-11T09:51:58Z
2022-11-11T09:51:58Z 2022-11 |
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| Type |
Article
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| Identifier |
2583-1321 (Online); 0019-5103 (Print)
http://nopr.niscpr.res.in/handle/123456789/60824 https://doi.org/10.56042/ijc.v61i11.68267 |
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| Language |
en
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| Publisher |
NIScPR-CSIR, India
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| Source |
IJC Vol.61(11) [Nov 2022]
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