<p>Solvent and catalyst free efficient chemoselective synthesis of 1,1-diacetate under visible light irradiation</p>
Online Publishing @ NISCAIR
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Title Statement |
<p>Solvent and catalyst free efficient chemoselective synthesis of 1,1-diacetate under visible light irradiation</p> |
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Added Entry - Uncontrolled Name |
Hote, Baliram S; Department of Chemistry, Maharashtra Udayagiri Mahavidyalaya Udgir, 413 517, Maharashtra, India Siddiqui, Tabassum A J; School of Chemical Sciences, Swami Ramanand Teerth Marathwada University, Nanded, 431 706, Maharashtra, India Pisal, Parshuram M; School of Chemical Sciences, Swami Ramanand Teerth Marathwada University, Nanded, 431 706, Maharashtra, India |
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Uncontrolled Index Term |
1,1-Diacetate, Visible light, Solvent- and catalyst free |
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Summary, etc. |
<p class="Default">One of the synthetic intermediates is used in many organic transformations. A method for highly efficient synthesis of 1,1-diacetate <strong>(3a-j)</strong> from mixture of various substituted benzaldehydes and acetic anhydride under solvent- and catalyst free using visible light irradiation (150 W tungsten lamp)has been developed. The main advantages of this protocol includes shorter reaction time, eco-friendly, mild reaction condition, easy work-up procedures, high yields of products, are the attractive features of the present methodology. All synthesized <strong>3a-j</strong> compounds were characterized by IR, <sup>1</sup>H NMR and mass spectral analysis.</p> |
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Publication, Distribution, Etc. |
Indian Journal of Chemistry (IJC) 2022-11-14 15:22:20 |
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Electronic Location and Access |
application/pdf http://op.niscair.res.in/index.php/IJC/article/view/68267 |
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Data Source Entry |
Indian Journal of Chemistry (IJC); ##issue.vol## 61, ##issue.no## 11 (2022): Indian Journal of Chemistry-(IJC) |
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Language Note |
en |
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