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Analytical method validation, dissipation and safety evaluation of combination fungicides fenamidone+ mancozeb and iprovalicarb+ propineb in/on tomato

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Title Analytical method validation, dissipation and safety evaluation of combination fungicides fenamidone+ mancozeb and iprovalicarb+ propineb in/on tomato
Not Available
 
Creator Yengkhom Bijen Kumar
Ahammed Shabeer TP
Manjusha Jadhav
Sandip Hingmire
Sujoy Saha
Kaushik Banerjee
Awadhesh Bahadur Rai
 
Subject Method validation
Dissipation and safety evaluation
Fenamidone + mancozeb
Iprovalicarb + propineb
Tomato
 
Description Not Available
Dissipation behavior and degradation kinetics of fenamidone + mancozeb (Sectin 60 WG) and iprovalicarb + propineb (Melody Duo 66.75 WP) in tomato were studied at recommended dose (RD) and double dose (DD) of application. The analysis of the field samples were carried out by employing liquid chromatography tandem mass spectrometry (LC–MS/MS) for fenamidone and iprovalicarb residues and gas chromatography mass spectrometry for mancozeb and propineb residues after thorough validation of the extraction methods. The dissipation of residues best followed 1st + 1st order for all the test fungicides. The half-life period for fenamidone, mancozeb, iprovalicarb and propineb were 2, 2, 1.5 and 2 days for RD and 3, 2.5, 2 and 3 days for DD, respectively. The pre-harvest intervals were not applicable for iprovalicarb, fenamidone and mancozeb (at RD) as the residues at 0 day were below maximum residue limit set by European Union, and it was 1 day for DD of iprovalicarb, 3.5 days for DD of fenamidone, 3 days for DD of mancozeb, 3 and 7 days for propineb at RD and DD, respectively. A PHI of 4 and 7 days are proposed for fenamidone + Mancozeb and iprovalicarb + propineb, respectively. Dietary exposure calculated for all the pesticides were safe on all the sampling days except for propineb residues for which it was safe after first day of the double dose application. The study will be useful for promoting effective residue management and safe use of these chemicals for controlling fungal diseases in tomato crop.
Not Available
 
Date 2020-07-29T16:14:04Z
2020-07-29T16:14:04Z
2020-01-20
 
Type Research Paper
 
Identifier Kumar, Y.B., Shabeer, T.P.A., Jadhav, M. et al. Analytical method validation, dissipation and safety evaluation of combination fungicides fenamidone + mancozeb and iprovalicarb + propineb in/on tomato. J Food Sci Technol 57, 2061–2069 (2020). https://doi.org/10.1007/s13197-020-04240-9
https://doi.org/10.1007/s13197-020-04240-9
http://krishi.icar.gov.in/jspui/handle/123456789/38512
 
Language English
 
Relation Not Available;
 
Publisher Springer