Multiresidue determination of 375 organic contaminants including pesticides, polychlorinated biphenyls and polyaromatic hydrocarbons in fruits and vegetables by gas chromatography-triple quadrupole mass spectrometry with introduction of semi-quantification approach
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Title |
Multiresidue determination of 375 organic contaminants including pesticides, polychlorinated biphenyls and polyaromatic hydrocarbons in fruits and vegetables by gas chromatography-triple quadrupole mass spectrometry with introduction of semi-quantification approach
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Creator |
Banerjee Kaushik, Utture S. Dasgupta S., Pradhan S. Kandaswamy C., Kulkarni S., Adsule P.G.
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Subject |
Multiresidue analysis of pesticides in fruits and vegetables
GC-MS/MS Method development and validation Semi-quantitative screening |
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Description |
Not Available
A residue analysis method for the simultaneous estimation of 349 pesticides, 11 PCBs and 15 PAHs extracted from grape, pomegranate, okra, tomato and onion matrices, was established by using a gas chromatograph coupled to an electron impact ionization triple quadrupole mass spectrometer (GC–EI-MS/MS). The samples were extracted by ethyl acetate and cleaned by dispersive solid phase extraction with PSA and/or GCB/C18 by the methods reported earlier. The GC–EI-MS/MS parameters were optimized for analysis of all the 375 compounds within a 40 min run time with limit of quantification for most of the compounds at 0.99 within the calibration linearity range of Not Available |
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Date |
2020-08-01T15:54:15Z
2020-08-01T15:54:15Z 2012-12-28 |
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Type |
Journal
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Identifier |
Banerjee Kaushik, Utture S. Dasgupta S., Pradhan S. Kandaswamy C., Kulkarni S., Adsule P.G. (2012). Multiresidue determination of 375 organic contaminants including pesticides, polychlorinated biphenyls and polyaromatic hydrocarbons in fruits and vegetables by gas chromatography-triple quadrupole mass spectrometry with introduction of semi-quantification approach. Journal of Chromatography A 1270: 283-295.
https://doi.org/10.1016/j.chroma.2012.10.066 http://krishi.icar.gov.in/jspui/handle/123456789/38881 |
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Language |
English
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Relation |
Not Available;
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Publisher |
Elsevier
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