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Optimization of a Modified QuEChERS Method for Multiresidue Analysis of Pharmaceuticals and Personal Care Products in Sewage and Surface Water by LC-MS/MS

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Title Optimization of a Modified QuEChERS Method for Multiresidue Analysis of Pharmaceuticals and Personal Care Products in Sewage and Surface Water by LC-MS/MS
Not Available
 
Creator Kachhawaha A.S., Nagarnaik P.M., Jadhav M.; Pudale, A.; Labhasetwar, P.K., Banerjee Kaushik
 
Subject Pharmaceuticals and personal care products in water
LC-MS/MS
Sewage and surface water
 
Description Not Available
A quick, sensitive multiresidue method was developed for the analysis of 19 multiclass pharmaceuticals and personal care products (PPCPs) in surface water and sewage water. The proposed modified QuEChERS method involved the extraction of water samples (10 mL) with acetonitrile (10 mL) after the addition of 1% acetic acid, 4 gmagnesium sulfate, and 0.2 g ammonium acetate, and was validated in distilled water, surface water, and sewagewater with respect to linearity, LOD and LOQ, precision, and accuracy. The LOD and LOQ varied within the ranges of 0.001–0.167 and 0.002–0.25 ng/mL, respectively. Recoveries of the target compounds ranged from 73 to 125%, with precision RSD values
Not Available
 
Date 2020-07-31T06:36:14Z
2020-07-31T06:36:14Z
2019-11-22
 
Type Journal
 
Identifier Kachhawaha A.S., Nagarnaik P.M., Jadhav M.; Pudale, A.; Labhasetwar, P.K., Banerjee Kaushik (2017). Optimization of a Modified QuEChERS Method for Multiresidue Analysis of Pharmaceuticals and Personal Care Products in Sewage and Surface Water by LC-MS/MS. Journal of AOAC International 100 (3): 592-597
https://doi.org/10.5740/jaoacint.17-0060
http://krishi.icar.gov.in/jspui/handle/123456789/38664
 
Language English
 
Relation Not Available;
 
Publisher Oxford University Press