Optimization of a Modified QuEChERS Method for Multiresidue Analysis of Pharmaceuticals and Personal Care Products in Sewage and Surface Water by LC-MS/MS
KRISHI: Publication and Data Inventory Repository
View Archive InfoField | Value | |
Title |
Optimization of a Modified QuEChERS Method for Multiresidue Analysis of Pharmaceuticals and Personal Care Products in Sewage and Surface Water by LC-MS/MS
Not Available |
|
Creator |
Kachhawaha A.S., Nagarnaik P.M., Jadhav M.; Pudale, A.; Labhasetwar, P.K., Banerjee Kaushik
|
|
Subject |
Pharmaceuticals and personal care products in water
LC-MS/MS Sewage and surface water |
|
Description |
Not Available
A quick, sensitive multiresidue method was developed for the analysis of 19 multiclass pharmaceuticals and personal care products (PPCPs) in surface water and sewage water. The proposed modified QuEChERS method involved the extraction of water samples (10 mL) with acetonitrile (10 mL) after the addition of 1% acetic acid, 4 gmagnesium sulfate, and 0.2 g ammonium acetate, and was validated in distilled water, surface water, and sewagewater with respect to linearity, LOD and LOQ, precision, and accuracy. The LOD and LOQ varied within the ranges of 0.001–0.167 and 0.002–0.25 ng/mL, respectively. Recoveries of the target compounds ranged from 73 to 125%, with precision RSD values Not Available |
|
Date |
2020-07-31T06:36:14Z
2020-07-31T06:36:14Z 2019-11-22 |
|
Type |
Journal
|
|
Identifier |
Kachhawaha A.S., Nagarnaik P.M., Jadhav M.; Pudale, A.; Labhasetwar, P.K., Banerjee Kaushik (2017). Optimization of a Modified QuEChERS Method for Multiresidue Analysis of Pharmaceuticals and Personal Care Products in Sewage and Surface Water by LC-MS/MS. Journal of AOAC International 100 (3): 592-597
https://doi.org/10.5740/jaoacint.17-0060 http://krishi.icar.gov.in/jspui/handle/123456789/38664 |
|
Language |
English
|
|
Relation |
Not Available;
|
|
Publisher |
Oxford University Press
|
|