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A liquid chromatographic method for determination of acetamiprid and buprofezin residues and their dissipation kinetics in paddy matrices and soil

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Title A liquid chromatographic method for determination of acetamiprid and buprofezin residues and their dissipation kinetics in paddy matrices and soil
Not Available
 
Creator Sujan Majumder
Somnath Mandal
Biswajit Majumder
Anindita Paul,
Tarun Paul,
Nandita Sahana
Prithusayak Mondal
 
Subject Persistence
Paddy
Consumer safety
Soil
Acetamiprid
Buprofezin
Insecticide residues
LC-MS/MS
Method validation
 
Description Not Available
The present study was conducted to investigate the residue status of two insecticides (acetamiprid and buprofezin) and their dissipation kinetics in three matrices viz. paddy grain, straw, and soil. The extraction procedure for residues of these two insecticides was executed using acetonitrile solvent. The analytical method was validated, which showed good linearity with the limit of quantification (LOQ) value of 0.01 and 0.02 mg kg−1 for acetamiprid and buprofezin, respectively. The recovery range was 79.67–98.33 % concerning all the matrices in both the insecticides. Acetamiprid (20% SP) and Buprofezin (25% SC) were applied separately in the paddy field in two doses: single dose (recommended dose) and double dose along with untreated control throughout the experiment. Residue analysis of these two insecticides in paddy (grain and straw) and soil was accomplished employing high-performance liquid chromatography (HPLC) with ultraviolet (UV) detector and confirmed by ultra-performance liquid chromatography (UPLC) coupled with mass spectrometry (UPLC-MS/MS). The dissipation data showed that acetamiprid exhibited higher dissipation in comparison with buprofezin. However, their persistence was found slightly higher in soil. The dissipation dynamics in the rice and soil were discussed with biological half-lives of both the insecticides. Consumer risk assessment study was also made considering its fate to the consumers.
Not Available
 
Date 2021-08-07T14:34:24Z
2021-08-07T14:34:24Z
2021-08-05
 
Type Research Paper
 
Identifier Not Available
Not Available
http://krishi.icar.gov.in/jspui/handle/123456789/53611
 
Language English
 
Relation Not Available;
 
Publisher Springer Nature