<p>Feasible pathways for the multi-dimensional synthesis of carboxylic acid from benzo-pyrone methyl ketone</p>
Online Publishing @ NISCAIR
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Title Statement |
<p>Feasible pathways for the multi-dimensional synthesis of carboxylic acid from benzo-pyrone methyl ketone</p> |
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Added Entry - Uncontrolled Name |
Yarva, Aruna ; Department of Humanities and Sciences, Hyderabad Institute of Technology and Management, Medchal, Hyderabad, Telangana 502 401, India Nagamalla, Lavanya ; Department of Humanities and Sciences, Hyderabad Institute of Technology and Management, Medchal, Hyderabad, Telangana 502 401, India K, Kavitha ; Department of Humanities and Sciences, Hyderabad Institute of Technology and Management, Medchal, Hyderabad, Telangana 502 401, India Department of Chemistry, Jawaharlal Nehru Technological University Hyderabad, College of Engineering, Kukatpally, Hyderabad, Telangana 500 085, India Pasula, Aparna ; Department of Chemistry, Jawaharlal Nehru Technological University Hyderabad, College of Engineering, Kukatpally, Hyderabad, Telangana 500 085, India Devulapally, Srikrishna ; Department of Chemistry, Jawaharlal Nehru Technological University Hyderabad, College of Engineering, Kukatpally, Hyderabad, Telangana 500 085, India Dubey, Pramod Kumar; Department of Chemistry, Jawaharlal Nehru Technological University Hyderabad, College of Engineering, Kukatpally, Hyderabad, Telangana 500 085, India |
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Uncontrolled Index Term |
Methyl ketone, Haloform reaction, Multi-dimensional synthesis, Phase transfer catalyst, Benzo-pyrone |
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Summary, etc. |
<p style="text-align: justify;">3-Acetyl coumarin derivatives are the key synthons to the numerous numbers of heterocyclic compound syntheses. Due to the wide spectrum applications of benzopyran derivatives in pharma, research, food technology and material science there is a multitude number of methodologies feasible to synthesize benzo pyrone heterocyclic derivatives. This article articulates the synthesis and molecular structure confirmation of oxidative product starting from methyl ketone compound by haloform reaction. Design of benign path ways for instance room temperature, reflux conditions and water bath mediated synthesis of desired compounds in expected yields is the foremost intent of the article. Solvent and catalyst optimization studies were carried to elevate the product yield and to precede the reaction in sustainable way. Furthermore compounds are confirmed by spectroscopic analytical methods such as <sup>1</sup>HNMR, <sup>13</sup>CNMR, IR and HRMS spectroscopy. This article paves the way to researchers to explore these analogues to explore disparate medicinal applications.</p> |
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Publication, Distribution, Etc. |
Indian Journal of Chemistry (IJC) 2023-01-19 15:48:46 |
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Electronic Location and Access |
application/pdf http://op.niscair.res.in/index.php/IJC/article/view/70352 |
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Data Source Entry |
Indian Journal of Chemistry (IJC); ##issue.vol## 62, ##issue.no## 1 (2023): Indian Journal of Chemistry-(IJC) |
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Language Note |
en |
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