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Feasible pathways for the multi-dimensional synthesis of carboxylic acid from benzo-pyrone methyl ketone

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Title Feasible pathways for the multi-dimensional synthesis of carboxylic acid from benzo-pyrone methyl ketone
 
Creator Yarva, Aruna
Nagamalla, Lavanya
K, Kavitha
Pasula, Aparna
Devulapally, Srikrishna
Kumar Dubey, Pramod
 
Subject Methyl ketone
Haloform reaction
Multi-dimensional synthesis
Phase transfer catalyst
Benzo-pyrone
 
Description 24-30
3-Acetyl coumarin derivatives are the key synthons to the numerous numbers of heterocyclic compound syntheses.Due to the wide spectrum applications of benzopyran derivatives in pharma, research, food technology and material science there is a multitude number of methodologies feasible to synthesize benzo pyrone heterocyclic derivatives. This article articulates the synthesis and molecular structure confirmation of oxidative product starting from methyl ketone compound by haloform reaction. Design of benign path ways for instance room temperature, reflux conditions and water bath mediated synthesis of desired compounds in expected yields is the foremost intent of the article. Solvent and catalyst optimization studies were carried to elevate the product yield and to precede the reaction in sustainable way. Furthermore compounds are confirmed by spectroscopic analytical methods such as 1H NMR, 13C NMR, IR and HRMS spectroscopy. This article paves the way to researchers to explore these analogues to explore disparate medicinal applications.
 
Date 2023-02-09T11:08:29Z
2023-02-09T11:08:29Z
2023-01
 
Type Article
 
Identifier 2583-1321 (Online); 0019-5103 (Print)
http://nopr.niscpr.res.in/handle/123456789/61380
https://doi.org/10.56042/ijc.v62i1.70352
 
Language en
 
Publisher NIScPR-CSIR, India
 
Source IJC Vol.62(01) [Jan 2023]