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Polarographic determination of heavy metal lead in waste water in Jaipur

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Title Polarographic determination of heavy metal lead in waste water in Jaipur
 
Creator Meena, Om Prakash
 
Description 112-116
Electro analytical Procedure was developed for the trace determination of heavy metal lead in waste water in Jaipur Rajasthan using Differential
pulse polarography. ELICO CL-362 POLAROGRAPHIC ANALYSER (Make: Elico) was used for measurement of current voltage relationship
(polarograms) on electrolyzing electro active analytes in polarographic cell. This apparatus has three electrode assembly, dropping mercury electrode
as working electrode, calomel as reference electrode and platinum as counter electrode. Dropping mercury electrode had the characteristics
m = 2.422 mg/sec, t = 2.5 sec and h = 60 cm, under the conditions of Pulse Amplitude 50 mV and 6 mV/S scan rate was used for
electroanalysis measurements. Electro analysis of lead in waste water was performed in 0.10 M KNO3as correlation of determination
(R2 = 0.999). Lead concentration in different water samples in Jaipur Rajasthan varies between 2.670 ppm to 5.757 ppm. Highest level of lead
is reported in Sanganerteshil(Summer season) (5.797 ppm).From this research showed that the developed electroanalysis of lead in waste water
using mercury drop electrode are accurate, precise, reproducible and inexpensive with acceptable the analysis of lead in waste water. This
method is simplicity of sample preparation and use of low cost reagents are the additional benefit.
 
Date 2023-11-28T08:22:22Z
2023-11-28T08:22:22Z
2023-11
 
Type Article
 
Identifier 0975-2412 (Online); 0971-7706 (Print)
http://nopr.niscpr.res.in/handle/123456789/62977
https://doi.org/10.56042/bvaap.v31i2.6384
 
Language en
 
Publisher NIScPR-CSIR,India
 
Source BVAAP Vol.31(2) [September 2023]